Data File D:\\AGLIENT 1260\\DATA\\20150209\\20150209 2015-02-09 09-21-52\\BIZ2015-209-DJL20.DSample Name: BIZ2015-209-DJL20=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 94Acq. Instrument : HY-LCMS-02 Location : Vial 62Injection Date : 2/9/2015 7:08:08 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150209\\20150209 2015-02-09 09-21-52\\100-1000MS+3MIN( 0.02%FA).MLast changed : 2/9/2015 9:21:52 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150206-1\\20150206 2015-02-06 14-52-11\\100-1000MS+ 3MIN(0.02%FA).M (Sequence Method)Last changed : 2/10/2015 9:03:38 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-102,40℃ Catalog No : HY-16562A Batch#149 A-RP-32 Additional Info : Peak(s) manually integrated DAD1 C, Sig=254,4 Ref=off (D:\\AGLIENT...0\\DATA\\20150209\\20150209 2015-02-09 09-21-52\\BIZ2015-209-DJL20.D) 1.348mAU140012001000800600400 1.60020000.511.5 1.70022.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.348 MM 0.0536 5320.06934 1654.29749 99.9529 2 1.600 MM 0.0483 7.25474e-1 2.50394e-1 0.0136 3 1.700 MM 0.0724 1.78241 4.101e-1 0.0335 Totals : 5322.57722 1654.95807 ===================================================================== *** End of Report ***HY-LCMS-02 2/10/2015 9:03:40 AM Li Shan(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20150209\\20150209 2015-02-09 09-21-52\\BIZ2015-209-DJL20.DSample Name: BIZ2015-209-DJL20=============================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 94Acq. Instrument : HY-LCMS-02 Location : Vial 62Injection Date : 2/9/2015 7:08:08 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150209\\20150209 2015-02-09 09-21-52\\100-1000MS+3MIN( 0.02%FA).MLast changed : 2/9/2015 9:21:52 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150206-1\\20150206 2015-02-06 14-52-11\\100-1000MS+ 3MIN(0.02%FA).M (Sequence Method)Last changed : 2/10/2015 9:05:03 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-102,40℃ Catalog No : HY-16562A Batch#149 A-RP-32 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150209\\20150209 2015-02-09 09-21-52\\BIZ2015-209-DJL20.D) ES-API, Pos, Sca 1.361100000080000060000040000020000000.511.522.53min HY-LCMS-02 2/10/2015 9:05:04 AM Li Shan(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20150209\\20150209 2015-02-09 09-21-52\\BIZ2015-209-DJL20.DSample Name: BIZ2015-209-DJL20MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.361 7107253 588.20 I 587.30 I 294.20 I*MSD1 SPC, time=1.325:1.416 of D:\\AGLIENT 1260\\DATA\\20150209\\20150209 2015-02-09 09-21-52\\BIZ2015-209-DJL20.D ES-API100806040200100200300400500600700800900m/z 587.3Max: 438219 294.2 *** End of Report ***HY-LCMS-02 2/10/2015 9:05:04 AM Li Shan(LCMS-02) 5.2 588.2Page 2 of 2
