MS Report from Instrument: LCMS-03 File ..\\Data\\20171106\\20171106\\CPK2017-N06-149.D Tgt Mass (CHM): Injection Date : 6 Nov 17 1:13 pm +0800 Seq. Line : 56 Sample Name : CPK2017-N06-149 Location : P1-E-04 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\20171106\\20171106\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20171106\\20171106\\1-POS-3MIN.M Catalog No : HY-16562A Batch#149 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off1000500000.5 DAD1 B, Sig=254,4 Ref=offmAU1000500000.5 ELS1 A, ELSD SignalmV200100000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7020000001000000000.511.5 Ion 624.2, MSD1 624.2,Target Mass 623.2 +H Positive, EIC=623.9:624.940002000000.511.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off22.5min1.3261.522.5min11.36211.2951.2951.257mAU1.522.5min1.2571.4631.4851.5571.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.26 0.01 3.74 4.20 0.25 587 1.30 0.01 1518.22 1598.79 99.75 587 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.26 0.02 5.35 4.60 0.42 587 1.30 0.02 1277.82 1359.51 99.54 587 1.46 0.01 0.07 0.10 0.01 303 1.49 0.01 0.07 0.09 0.01 303 1.56 0.02 0.36 0.25 0.03 303 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.33 0.06 11413022.00 2934099.75 100.00 587LCMS-03 11/6/2017 15:49:14 SYSTEMPage1 of3MS Report from Instrument: LCMS-03Ret. Time: 1.33 <<<< POSITIVE SPECTRA >>>>*ES-API Positive587.2294.2250000200000150000100000500000100200300400500600700800900m/zLCMS-03 11/6/2017 15:49:14 SYSTEMPage2 of3MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 11/6/2017 15:49:14 SYSTEMPage3 of3
