Data File D:\\CHEM\\DATA\\20160623\\20160623 2016-06-23 11-29-36\\027-2401.DSample Name: JS3527-007-5_0=====================================================================Acq. Operator : SW(HPLC-04) Seq. Line : 24Acq. Instrument : 1 Location : Vial 27 Injection Date : 6/23/2016 6:06:09 PM Inj : 1 Inj Volume : 5.0 µlDifferent Inj Volume from Sequence Actual Inj Volume : 1.0 µlAcq. Method : D:\\CHEM\\DATA\\20160623\\20160623 2016-06-23 11-29-36\\HY-331_14-H01EE08,225NM. MLast changed : 6/23/2016 4:44:50 PM by SW(HPLC-04)Analysis Method : D:\\CHEM\\METHODS\\OZ,85-ETOH,210NM.MLast changed : 6/24/2016 8:41:23 AM by SW(HPLC-04) (modified after loading)Catalog No : HY-14881 Batch#20752 C-NP-17 Additional Info : Peak(s) manually integrated VWD1 A, Wavelength=225 nm (D:\\CHEM\\DATA\\20160623\\20160623 2016-06-23 11-29-36\\027-2401.D)mAU 3020100-10-20-30-4002.557.51012.51517.5min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier: : 1.0000Dilution: : 1.0000Use Multiplier & Dilution Factor with ISTDs No peaks found ===================================================================== *** End of Report *** 1 6/24/2016 8:42:23 AM SW(HPLC-04)Page 1 of 1
Data File D:\\CHEM\\DATA\\20160623\\20160623 2016-06-23 11-29-36\\026-2501.DSample Name: JS3527-007-5=====================================================================Acq. Operator : SW(HPLC-04) Seq. Line : 25Acq. Instrument : 1 Location : Vial 26 Injection Date : 6/23/2016 6:27:37 PM Inj : 1 Inj Volume : 5.0 µlDifferent Inj Volume from Sequence Actual Inj Volume : 1.0 µlAcq. Method : D:\\CHEM\\DATA\\20160623\\20160623 2016-06-23 11-29-36\\HY-331_14-H01EE08,225NM. MLast changed : 6/23/2016 4:44:50 PM by SW(HPLC-04)Analysis Method : D:\\CHEM\\METHODS\\OZ,85-ETOH,210NM.MLast changed : 6/24/2016 8:41:23 AM by SW(HPLC-04) (modified after loading)Catalog No : HY-14881 Batch#20752 C-NP-17 Additional Info : Peak(s) manually integrated VWD1 A, Wavelength=225 nm (D:\\CHEM\\DATA\\20160623\\20160623 2016-06-23 11-29-36\\026-2501.D) 14.484mAU 350300250200150100500-5002.557.51012.51517.5min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier: : 1.0000Dilution: : 1.0000Use Multiplier & Dilution Factor with ISTDs Signal 1: VWD1 A, Wavelength=225 nm Peak RetTime Type Width Area Height Area # [min] [min] mAU *s [mAU ] %----|-------|----|-------|----------|----------|--------| 1 14.484 BB 0.4324 1.09444e4 391.53867 100.0000 Totals : 1.09444e4 391.53867 ===================================================================== *** End of Report *** 1 6/24/2016 8:41:24 AM SW(HPLC-04)Page 1 of 1
Data File D:\\CHEM\\DATA\\20160623\\20160623 2016-06-23 11-29-36\\065-2801.DSample Name: JS3527-007-5_MIX=====================================================================Acq. Operator : SW(HPLC-04) Seq. Line : 28Acq. Instrument : 1 Location : Vial 65 Injection Date : 6/23/2016 7:32:08 PM Inj : 1 Inj Volume : 5.0 µlDifferent Inj Volume from Sequence Actual Inj Volume : 1.0 µlAcq. Method : D:\\CHEM\\DATA\\20160623\\20160623 2016-06-23 11-29-36\\HY-331_14-H01EE08,225NM. MLast changed : 6/23/2016 4:44:50 PM by SW(HPLC-04)Analysis Method : D:\\CHEM\\METHODS\\OZ,85-ETOH,210NM.MLast changed : 6/24/2016 8:41:23 AM by SW(HPLC-04) (modified after loading)Catalog No : HY-14881 Batch#20752 C-NP-17 Additional Info : Peak(s) manually integrated VWD1 A, Wavelength=225 nm (D:\\CHEM\\DATA\\20160623\\20160623 2016-06-23 11-29-36\\065-2801.D) 13.321 14.558mAU 600500400300200100002.557.51012.51517.5min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier: : 1.0000Dilution: : 1.0000Use Multiplier & Dilution Factor with ISTDs Signal 1: VWD1 A, Wavelength=225 nm Peak RetTime Type Width Area Height Area # [min] [min] mAU *s [mAU ] %----|-------|----|-------|----------|----------|--------| 1 13.321 BV 0.3931 1.34546e4 531.18188 42.0466 2 14.558 VV 0.43 1.85447e4 658.30133 57.9534 Totals : 3.19994e4 11.48322 ===================================================================== *** End of Report *** 1 6/24/2016 8:42:01 AM SW(HPLC-04)Page 1 of 1